Faculty-in-Charge: Prof. S S Singh
Phone:
Email: tga_crf@iitism.ac.in
Make: NETZSCH
Model: STA 2500 with QMS 505 Aeolos Coupling
The NETZSCH STA 2500 Regulus is a Simultaneous Thermal Analyzer (STA) designed for high-reliability, cost-effective measurement of materials. It combines Thermogravimetric Analysis (TGA) and Differential Thermal Analysis (DTA/DSC), allowing for simultaneous measurement of mass changes and caloric events on the same sample under identical conditions.
Key features include a top-loading, vertical, and differential balance system. This unique differential design cancels out buoyancy and convection effects, eliminating the need for time-consuming baseline runs and ensuring stable measurements with a high thermogravimetric resolution of 0.03 micro gram. .
The instrument operates up to 1100C and supports a wide range of atmospheres, including inert, oxidizing, and vacuum, controlled by Quadrupole Mass Spectrometer (QMS). Its top-loading design is also ideal for coupling to Evolved Gas Analysis (EGA) systems like Mass Spectrometry (MS) to analyze the gases released during thermal treatment.
| Instrument Design | |
|---|---|
| Model | STA 2500 Regulus |
| Design | Top-loading, vertical & differential balance |
| Furnace Data | |
| Temperature Range | RT to 1100°C |
| Heating Rate | 0.001 to 100 K/min (depending on the furnace) |
| Temperature Precision (Repeatability) | 0.3 K |
| Motorized Furnace Hoist | Single hoist |
| Balance and Sensor Data | |
| Balance Design | Differential balance system |
| Weighing Range | ± 250 mg, max. sample load 1 g |
| Thermogravimetric Resolution | 0.03 μg |
| Thermocouple | Type S |
| Atmosphere | |
| Vacuum Tightness | 10-4 mbar (10-2 Pa), depending on the evacuation system |
| Gas Atmospheres | Inert, oxidizing, vacuum |
| Gas Control | Built-in mass flow controllers |
| Robot System | |
| Automatic Sample Changer (ASC) | Optionally available for 20 crucibles |